Ti
tio2agentsSEMITI
Menu
Applications · Plastics

TiO2 for Plastic Masterbatch

White masterbatch concentrates for PE, PP, ABS, PS film and injection molding — typically 50–70% TiO2 loading.

Plastic masterbatch is the second-largest TiO2 application after architectural coatings, accounting for roughly 25% of global demand. Compounders produce concentrated "white masterbatch" — typically 50–70% TiO2 in a polyolefin carrier (PE wax, PE base, EVA, or compatible polymer) — which is then let down to 1–5% in the final plastic part.

The performance profile demanded of masterbatch-grade TiO2 differs sharply from coatings-grade TiO2. Three properties dominate:

1. Thermal stability — extrusion temperatures range from 180–230°C for LDPE film up to 280–300°C for engineering plastics. The TiO2 surface treatment must survive this without yellowing or evolving moisture that creates surface defects.

2. Extrusion behavior — high-loading masterbatch (60–70%) puts enormous demand on dispersion. Poor dispersion shows up as "fish eyes," nozzle deposits, and screen blinding. Surface treatment must wet quickly into the carrier polymer at melt temperature.

3. Compatibility with downstream additives — masterbatch typically goes into film with slip agents (erucamide, oleamide), antiblocks (talc, silica), antioxidants (Irganox 1010), UV stabilizers (HALS, UV absorbers). The TiO2 surface treatment must not interfere with these — particularly important is no amine-blocking behavior that would degrade HALS efficiency.

SEMITI's masterbatch lineup spans the performance/cost range: - SEMITI 960 — chloride rutile with amine-compatible surface treatment, thermal stability to 300°C (engineering plastics: ABS, PA, PC blends) - SEMITI 996 — universal grade, thermal stability to 280°C (PE, PP, PVC — covers 80% of commodity masterbatch) - SEMITI 2310 — direct alternative to Kronos 2310, universal plastics grade - SEMITI 2190 — premium grade for outdoor / weatherable applications (PVC siding, agricultural film)

Performance requirements

Thermal stability (yellowing)Δb* ≤ 1.5 after 5 min at 280°C (commodity); ≤ 2.0 at 300°C (engineering)
Volatiles at 105°C≤ 0.30% — higher values cause surface defects in film extrusion
Loss on ignition (105–800°C)≤ 0.50%
Dispersion (fish eye)≤ 5 visible defects per 100 cm² in 50 μm PE blown film at 50% loading
Screen pack life≥ 2 hr at 70% loading, 25 kg/hr, 90 mesh screen
Compatibility with HALSNo measurable HALS degradation in 1000 hr QUV at 1% HALS + 2% TiO2 in LLDPE film

Dosage guidance

Two-stage calculation: (1) masterbatch composition, (2) finished product loading. Masterbatch composition (TiO2 % in concentrate): - Standard commodity white MB: 50% TiO2 + 47% LDPE carrier + 3% dispersant package - Premium MB: 60% TiO2 + 37% carrier + 3% dispersant - Maximum-load MB: 70–75% TiO2 + 22–27% carrier + 3–5% dispersant — limits at carrier flow Finished product TiO2 (after letdown): - White PE film for packaging: 2–4% TiO2 - White PP molded parts: 1–3% TiO2 - Opaque PVC siding: 3–6% TiO2 - White ABS / PC body parts: 2–5% TiO2 - Outdoor agricultural film: 1–2% TiO2 + UV absorber package Most masterbatch makers run 50/50 or 60/40 MB. The choice depends on dosing equipment precision — 50/50 lets the converter dose at 5% finished product (good for gravimetric feeders); 60/40 lets them dose at 4% (better for tight cost control on big runs).

Dispersion / processing notes

Twin-screw extruder is standard — typical setup: L/D 36–44, kneading blocks at zones 3–5, vacuum venting at zones 6–7 to remove residual moisture. For 60%+ loading, add a side feeder at zone 4 to introduce TiO2 separately from the carrier. Screw speed 300–500 rpm. Output temperature should not exceed the TiO2 surface treatment's stability limit (check spec — usually 230–250°C for commodity grades, 280°C+ for premium). For final-product extrusion of films, a 60-mesh + 120-mesh + 200-mesh screen pack catches any oversize agglomerates from the masterbatch.

Formulation tips

  • Pair TiO2 with 1–3% calcium stearate or PE wax as primary dispersant — wets the pigment surface, lowers compound viscosity
  • For engineering plastics (ABS, PC, PA), use amine-treated grades (SEMITI 960) — avoids HALS antagonism
  • Pre-dry TiO2 to <0.2% moisture before high-load (>60%) compounding — surface moisture causes splay in injection molding
  • For outdoor / weatherable masterbatch, layer in 0.3–0.5% HALS + 0.2% UV absorber on top of the TiO2 to extend service life 3–5x
  • Test masterbatch by extruding film at 100–150 g/m² and counting visible defects under transmitted light — better than viscosity-based dispersion tests

Common pitfalls

Failure modes we've seen in customer trials — worth checking before scale-up.

  • ×Using coating-grade TiO2 (SEMITI 902, designed for solvent/water) in masterbatch — the surface treatment moisture (1–2%) creates splay defects in injection molding
  • ×Mixing chloride + sulfate TiO2 in the same masterbatch — different surface chemistries cause inconsistent dispersion, fish-eye defects
  • ×Skipping the vacuum vent on the extruder when running >60% loading — residual moisture in the TiO2 surface treatment causes voids in the strand
  • ×Overheating engineering plastics MB (>320°C) — even premium TiO2 grades yellow at this temperature, and the carrier polymer degrades
  • ×Forgetting that nano-TiO2 (SEMITI NANO-30) is for personal care, NOT plastics — nano TiO2 in plastics causes photocatalytic polymer degradation

Common questions

What's the highest TiO2 loading I can run in a 50:1 L/D twin-screw?+
Practical limit is around 75% in PE carrier with a strong dispersant package. Above 75%, the compound becomes too viscous to flow through the die. Most commercial 'high-load' MBs are 70%. Below 50% loading the masterbatch is uneconomic — the carrier polymer dilutes the active too much.
Can I use SEMITI 996 in PE blown film masterbatch?+
Yes — SEMITI 996 is one of our highest-volume MB grades. Typical recipe: 50% SEMITI 996 + 47% LDPE base + 1.5% calcium stearate + 1.5% PE wax. Runs cleanly on standard twin-screw (Coperion ZSK 40 / 50 class) at 300–400 kg/hr.
How does SEMITI 960 compare with Ti-Pure R-960 for ABS masterbatch?+
Direct technical equivalent. We've validated SEMITI 960 against R-960 in 3 ABS converters in India and Vietnam — Δb* difference < 0.5 after 280°C, 5 min hold. Cost difference: SEMITI 960 lands 35–40% cheaper into Mumbai/Ho Chi Minh.
Does TiO2 affect food contact compliance?+
TiO2 is approved for food contact under FDA 21 CFR 178.3297, EU 10/2011 (no SML), China GB 9685-2016, and most national regulations. Migration testing typically required for liquid food contact at >2% loading — we provide migration test certificates on request.

Need help picking a grade for plastic masterbatch?

Send us your reference grade, formulation type, or competitor TDS. We'll respond with the SEMITI match + sample within 48 hours.